Basics of Analytical Chemistry and Chemical Equilibria 2e By Brian Tissue

Introducing Basics of Analytical Chemistry and Chemical Equilibria, 2e by Brian M. Tissue

I am pleased to present an in-depth introduction to Basics of Analytical Chemistry and Chemical Equilibria: A Quantitative Approach, Second Edition, authored by 「Brian M. Tissue」, Associate Professor of Chemistry at Virginia Tech, Blacksburg, VA. This exceptional textbook—published in 2023 by John Wiley & Sons—spans 496 pages and is tailored for advanced undergraduates, graduate students, and researchers in analytical chemistry, biochemistry, environmental science, chemical engineering, and related fields.

Overview and Pedagogical Design

This new edition distinguishes itself with several key enhancements:

• A brand-new chapter on 「molecular structure determination」, equipping readers to interpret data from IR, NMR, and mass spectrometry.
• 「Revised and expanded discussion」 of chemical instrumentation—reflecting recent technological advances in analytical methods.
• Interactive 「“You-Try-It” exercises」 interspersed throughout the chapters, designed to promote active learning and practical mastery.
• A comprehensive 「companion website」, offering end-of-chapter solutions, spreadsheet templates for calculations, a glossary of key terms, and more resources to facilitate learning.

Structure and Content Highlights

The book is methodically organized into three parts, each building on fundamental principles toward advanced applications:

Part I – Quantitative Analysis Using Reactions That Go to “Completion”

• 「Chapter 1: Making Measurements」 Explores laboratory best practices, calibration, uncertainty, statistical analysis, and precision—laying the groundwork for robust quantitative work.

• 「Chapter 2: Sample Preparation, Extractions, and Chromatography」 Details sampling strategies, extraction principles, solvent systems, solid-phase extraction, and preparative chromatography—crucial for obtaining reliable results.

• 「Chapter 3: Classical (Wet-Chemical) Methods」 Describes gravimetric analysis, titrations, coulometry, and stoichiometry-based approaches—foundational methods still used for validation and high-concentration analyses.

• 「Chapter 4: Molecular Spectroscopy」 Introduces UV/Vis absorption, fluorescence spectroscopy, Beer-Lambert law, and molecular transitions—fundamental analytical tools in many laboratories.

Part II – Reactions That Do Not Go to “Completion”: Equilibria in Aqueous Solutions

• 「Chapter 5: Acid–Base Equilibria and Activity」 Covers definitions of acids/bases, activity and ionic strength, equilibrium constants, and practical calculations—critical in buffer and titration studies.

• 「Chapter 6: Buffer Solutions and Polyprotic Acids」 Examines Henderson–Hasselbalch, alpha-fraction plots, and pH behavior of polyprotic systems—vital for titration and buffering considerations.

• 「Chapter 7: Metal–Ligand Complexation」 Explores stability constants, stepwise and cumulative equilibria, and masking agents—relevant in complexometric titrations and spectroscopic analysis.

• 「Chapter 8: Precipitation Equilibria」 Discusses solubility products (K_sp), common-ion and ionic-strength effects, and environmental implications such as contaminant behavior in water.

Part III – Instrumental Methods and Analytical Separations

• 「Chapter 9: Electroanalytical Chemistry」 Covers redox fundamentals, electrochemical cells, potentiometry, voltammetry, and analytical applications of electrochemistry.

• 「Chapter 10: Atomic Spectrometry」 Describes instrumentation and principles of AAS, AES, ICP-MS; application of such techniques to elemental analysis and interference management.

• 「Chapter 11: Molecular Structure Determination」 The new addition offering insights into FTIR, NMR, and mass spectrometry for elucidating structures—key for qualitative analysis.

• 「Chapter 12: Analytical Separations」 Focuses on separation techniques: TLC, HPLC, GC, electrophoresis, instrumentation, and interpretation for complex sample analysis.

An 「Epilogue」 provides closure and guidance for next steps in analytical development, emphasizing conceptual integration.

Instructor and Student Resources

Beyond the printed volume, the companion website (available at Wiley’s site for this text) includes:

• Detailed 「solutions」 to practice problems
• 「Spreadsheet templates」 for hands-on exercises
• A 「glossary」 for rapid reference to technical terminology

These resources are especially beneficial for instructors designing coursework or for independent study by ambitious researchers and students.

Why This Text Stands Out

• 「Integration of Theory and Practice」: The progression from measurement fundamentals to advanced techniques enables readers to build a cohesive analytical framework.
• 「Active Learning」: The “You-Try-It” segments encourage deliberate practice, promoting deeper understanding beyond passive reading.
• 「Modern Instrumentation Focus」: The second edition’s updates ensure readers learn about current tools and strategies in analytical labs.
• 「Rigorous yet Accessible」: The book maintains academic rigor suitable for research training, yet presents material clearly and logically.
• 「Broad Relevance」: Spanning traditional wet-chemical methods to cutting-edge spectroscopy and separations, the text supports interdisciplinary applications in chemistry, biology, environmental science, and engineering.

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Basics of Analytical Chemistry and Chemical Equilibria 2e

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